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Example of an <t>operando</t> depth profile measurement obtained with the BLiX CMXRF spectrometer. a) CMXRF spectra at three selected depth positions: at the HOPG window, in the NMC cathode and in the Cu back contact. b) 2D map of the CMXRF spectra in the energetic region between the Ar K and Cu K fluorescence lines as a function of relative depth (intensity is given in cps). c) Depth profiles of the individual fluorescence peaks are the net peak intensities as a function of relative depth. The different layers of the NMC coin cell are attributed to the elemental signals.
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Example of an <t>operando</t> depth profile measurement obtained with the BLiX CMXRF spectrometer. a) CMXRF spectra at three selected depth positions: at the HOPG window, in the NMC cathode and in the Cu back contact. b) 2D map of the CMXRF spectra in the energetic region between the Ar K and Cu K fluorescence lines as a function of relative depth (intensity is given in cps). c) Depth profiles of the individual fluorescence peaks are the net peak intensities as a function of relative depth. The different layers of the NMC coin cell are attributed to the elemental signals.
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Example of an <t>operando</t> depth profile measurement obtained with the BLiX CMXRF spectrometer. a) CMXRF spectra at three selected depth positions: at the HOPG window, in the NMC cathode and in the Cu back contact. b) 2D map of the CMXRF spectra in the energetic region between the Ar K and Cu K fluorescence lines as a function of relative depth (intensity is given in cps). c) Depth profiles of the individual fluorescence peaks are the net peak intensities as a function of relative depth. The different layers of the NMC coin cell are attributed to the elemental signals.
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Example of an <t>operando</t> depth profile measurement obtained with the BLiX CMXRF spectrometer. a) CMXRF spectra at three selected depth positions: at the HOPG window, in the NMC cathode and in the Cu back contact. b) 2D map of the CMXRF spectra in the energetic region between the Ar K and Cu K fluorescence lines as a function of relative depth (intensity is given in cps). c) Depth profiles of the individual fluorescence peaks are the net peak intensities as a function of relative depth. The different layers of the NMC coin cell are attributed to the elemental signals.
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Example of an <t>operando</t> depth profile measurement obtained with the BLiX CMXRF spectrometer. a) CMXRF spectra at three selected depth positions: at the HOPG window, in the NMC cathode and in the Cu back contact. b) 2D map of the CMXRF spectra in the energetic region between the Ar K and Cu K fluorescence lines as a function of relative depth (intensity is given in cps). c) Depth profiles of the individual fluorescence peaks are the net peak intensities as a function of relative depth. The different layers of the NMC coin cell are attributed to the elemental signals.
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Example of an operando depth profile measurement obtained with the BLiX CMXRF spectrometer. a) CMXRF spectra at three selected depth positions: at the HOPG window, in the NMC cathode and in the Cu back contact. b) 2D map of the CMXRF spectra in the energetic region between the Ar K and Cu K fluorescence lines as a function of relative depth (intensity is given in cps). c) Depth profiles of the individual fluorescence peaks are the net peak intensities as a function of relative depth. The different layers of the NMC coin cell are attributed to the elemental signals.

Journal: Small (Weinheim an Der Bergstrasse, Germany)

Article Title: Operando Measurement of Transition Metal Deposition in a NMC Li‐Ion Battery Using Laboratory Confocal Micro‐X‐ray Fluorescence Spectroscopy

doi: 10.1002/smll.202502460

Figure Lengend Snippet: Example of an operando depth profile measurement obtained with the BLiX CMXRF spectrometer. a) CMXRF spectra at three selected depth positions: at the HOPG window, in the NMC cathode and in the Cu back contact. b) 2D map of the CMXRF spectra in the energetic region between the Ar K and Cu K fluorescence lines as a function of relative depth (intensity is given in cps). c) Depth profiles of the individual fluorescence peaks are the net peak intensities as a function of relative depth. The different layers of the NMC coin cell are attributed to the elemental signals.

Article Snippet: I. Mantouvalou , L. Mathies , K. Frenzel , Y. Wagener , L. J. Bauer , D. Grötzsch , M. Müller , B. Kanngießer , M. Winter , S. Nowak , A. Jonas , B. Beckhoff , Operando Measurement of Transition Metal Deposition in a NMC Li‐Ion Battery Using Laboratory Confocal Micro‐X‐ray Fluorescence Spectroscopy .

Techniques: Operando Spectroscopy, Fluorescence

a) Photo of the BLiX CMXRF setup with potentiostat which was used for the operando measurements. b) Detail of the sample holder with 4 coin cells inside the measurement chamber. c) Picture from the side. The tips of both polycapillary lenses can be seen as well as the holder with the coin cell, demonstrating the small working distance.

Journal: Small (Weinheim an Der Bergstrasse, Germany)

Article Title: Operando Measurement of Transition Metal Deposition in a NMC Li‐Ion Battery Using Laboratory Confocal Micro‐X‐ray Fluorescence Spectroscopy

doi: 10.1002/smll.202502460

Figure Lengend Snippet: a) Photo of the BLiX CMXRF setup with potentiostat which was used for the operando measurements. b) Detail of the sample holder with 4 coin cells inside the measurement chamber. c) Picture from the side. The tips of both polycapillary lenses can be seen as well as the holder with the coin cell, demonstrating the small working distance.

Article Snippet: I. Mantouvalou , L. Mathies , K. Frenzel , Y. Wagener , L. J. Bauer , D. Grötzsch , M. Müller , B. Kanngießer , M. Winter , S. Nowak , A. Jonas , B. Beckhoff , Operando Measurement of Transition Metal Deposition in a NMC Li‐Ion Battery Using Laboratory Confocal Micro‐X‐ray Fluorescence Spectroscopy .

Techniques: Operando Spectroscopy